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A novolac-based polytriazole (NPTA) resin was synthesized using 4,4′-diazidomethylbiphenyl and a propargylated novolac resin through catalyst-free click polymerization. Differential scanning calorimetry and Fourier transform infrared analysis results demonstrate that the NPTA resin can be cured at 80°C. The glass transition temperature of the cured NPTA-88 resin is 202°C. The thermal degradation temperature of the cured NPTA resin is 352°C under nitrogen. The composite of the resin exhibits good mechanical property.