MULTINUCLEAR NMR SPECTROSCOPIC CHARACTERIZATION OF VANADIUM(V) ALKYLPEROXO COMPLEXES VO(OOtBu)k(OnBu)3−k, WHERE k = 1, 2, 3


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Abstract

Using 51V, 17O, 13C and 1H NMR spectroscopy, vanadium(V) alkylperoxo complexes VO(OOtBu)k(OnBu)3-k, where k = 1, 2 and 3, were characterized in the reaction of VO(OnBu)3 with tBuOOH in CH2Cl2.

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