Photochromic Dihetarylethenes: XX.* Synthesis and Photochromic Properties of Dithienylethenes with a Fixed Conformation


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Abstract

A procedure was developed for the synthesis of bis(2,5-dimethyl-3-thienyl)ethenes with partially fixed molecular conformation, and their photochromic properties in solution were studied. The structure of photochromic 1-(2,5-dimethyl-3-thienyl)-7,9-dimethyl-5,6-dihydrothieno[3′,4′: 3,4]pyrido[1,2-c][1,3]oxazol-3-one, as well as of 1-(2,5-dimethyl-3-thienyl)-7,9-dimethylthieno[3′,4′: 3,4]pyrido[1,2-c][1,3]oxazol-3-one possessing no photochromic properties, was determined by X-ray analysis.

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